Wednesday, February 15, 2012
Working with silica update
Silicon wafers were placed in an oven at 900 degrees C for 3 hours in order to apply a thermal oxide layer for SiO2. They were then cut using a diamond tipped etching tool and have been running tests using the modified Langmuir-trough setup to observe the film on the surface. So far have used 100 and 200 nm sphere solutions with films that are almost fully complete after examination with the naked eye. However, there are still a few spots which should not be bare and therefore we will be working on changing the speed of the trough "floaters", which maintain the surfactant concentration near the surface of the substrate as it's being withdrawn. My hope is that by increasing the speed and making sure that the substrate does not come into contact with the floaters, the increased surfactant concentration near the substrate surface will allow for a more even coating of the spheres. If this does not increase the uniformity of the film then another option would be to increase the SDS concentration in an attempt to increase the concentration of individual spheres (non-aggregated) near the liquid-air interface.
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